

                             INSTRUMENT CONTROL PARAMETERS:    GCMS
                             --------------------------------------

   C:\MSDCHEM\1\METHODS\DB225-FAME-012414.M
      Fri Mar 28 21:58:42 2014

Control Information
------- -----------

Sample Inlet      :  GC
Injection Source  :  GC ALS
Mass Spectrometer :  Enabled

=============================================================================
                                6890 GC METHOD
=============================================================================


OVEN
   Initial temp:  64 'C (On)               Maximum temp:  240 'C
   Initial time:  2.00 min                 Equilibration time:  2.00 min
   Ramps:
      #  Rate  Final temp  Final time
      1 60.00      184        0.00
      2  3.00      205        0.00
      3  1.00      210        0.00
      4  5.00      235        2.00
      5   0.0(Off)
   Post temp:  240 'C
   Post time:  6.00 min
   Run time:  23.00 min


FRONT INLET (SPLIT/SPLITLESS)           BACK INLET (SPLIT/SPLITLESS)
   Mode:  Splitless                        Mode:  Split
   Initial temp:  225 'C (On)              Initial temp:  50 'C (Off)
   Pressure:  25.54 psi (On)               Pressure:  0.00 psi (Off)
   Purge flow:  15.1 mL/min                Total flow:  45.0 mL/min
   Purge time:  1.00 min                   Gas saver:  Off
   Total flow:  20.1 mL/min                Gas type:  Helium
   Gas saver:  On
   Saver flow:  15.0 mL/min
   Saver time:  2.00 min
   Gas type:  Helium


COLUMN 1                                COLUMN 2
   Capillary Column                        Capillary Column
   Model Number:  J&W 122-2932             Model Number:  Agilent 160-2615
   DB-225ms                                MSD Backflush Restrictor
   Max temperature:  240 'C                Max temperature:  360 'C
   Nominal length:  30.0 m                 Nominal length:  4.0 m
   Nominal diameter:  250.00 um            Nominal diameter:  180.00 um
   Nominal film thickness:  0.25 um        Nominal film thickness:  0.00 um
   Mode:  ramped flow                      Mode:  constant flow
   Initial flow:  2.5 mL/min               Initial flow:  2.0 mL/min
   Initial time:  0.00 min                 Nominal init pressure:  8.28 psi
      #  Rate  Final flow  Final time      Average velocity:  142 cm/sec
      1   0.0(Off)                         Inlet:  Aux 5 Pressure Controller
   Post flow:  0.1 mL/min                  Outlet:  MSD
   Nominal init pressure:  25.55 psi       Outlet pressure:  vacuum
   Average velocity:  47 cm/sec
   Inlet:  Front Inlet
   Outlet:  Front Detector
   Outlet pressure:  2.00 psi


FRONT DETECTOR (FID)                    BACK DETECTOR (NO DET)
   Temperature:  110 'C (On)
   Hydrogen flow:  40.0 mL/min (Off)
   Air flow:  450.0 mL/min (Off)
   Mode:  Constant makeup flow
   Makeup flow:  45.0 mL/min (Off)
   Makeup Gas Type: Helium
   Flame:  Off
   Electrometer:  Off
   Lit offset:  2.0


SIGNAL 1                                SIGNAL 2
   Data rate:  20 Hz                       Data rate:  20 Hz
   Type:  front detector                   Type:  front detector
   Save Data:  On                          Save Data:  Off
   Zero:  0.0 (Off)                        Zero:  0.0 (Off)
   Range:  0                               Range:  0
   Fast Peaks:  Off                        Fast Peaks:  Off
   Attenuation:  0                         Attenuation:  0


COLUMN COMP 1                           COLUMN COMP 2
   Derive from front detector              Derive from front detector


THERMAL AUX 2                           AUX PRESSURE 3
   Use:  MSD Transfer Line Heater          Description:
   Description:  MSD                       Gas Type:  Helium
   Initial temp:  240 'C (On)              Initial pressure:  0.00 psi (Off)
   Initial time:  0.00 min
      #  Rate  Final temp  Final time
      1   0.0(Off)


AUX PRESSURE 4                          AUX PRESSURE 5
   Description:                            Description:  Backflush Aux5
   Gas Type:  Helium                       Gas Type:  Helium
   Initial pressure:  0.00 psi (Off)       Driving Column 2
                                           Initial pressure:  8.28 psi (On)


VALVES                                  POST RUN
   Valve 5  Switching Off                  Post Time: 6.00 min
      Description:                         Oven Temperature: 240 'C
                                           Column 1 Flow: 0.1 mL/min
                                           Column 2 Flow: 6.0 mL/min


TIME TABLE
   Time       Specifier                     Parameter & Setpoint




                               GC Injector


     Front Injector:
        Sample Washes                 0
        Sample Pumps                  3
        Injection Volume           1.00 microliters
        Syringe Size               10.0 microliters
        PreInj Solvent A Washes       0
        PreInj Solvent B Washes       0
        PostInj Solvent A Washes      3
        PostInj Solvent B Washes      3
        Viscosity Delay               1 seconds
        Plunger Speed              Fast
        PreInjection Dwell         0.02 minutes
        PostInjection Dwell        0.02 minutes


     Back Injector:
No parameters specified

 Column 1 Inventory Number : AB001
 Column 2 Inventory Number : Restrictor

                                MS ACQUISITION PARAMETERS


General Information
------- -----------

Tune File                : atune.u
Acquistion Mode          : Scan/SIM


MS Information
-- -----------

Solvent Delay            : 4.00 min

EMV Mode                 : Relative
Relative Voltage         : 0
Resulting EM Voltage     : 2376

[Scan Parameters]

Low Mass                 : 50.0
High Mass                : 400.0
Threshold                : 10
Sample #                 : 0       A/D Samples    1
[Sim Parameters]

GROUP 1
Group ID                 : All FAMES
Resolution               : Low
Plot 1 Ion               : 55.10
Ions/Dwell In Group      (  Mass,  Dwell) (  Mass,  Dwell) (  Mass,  Dwell) 
                         ( 55.10,      8) ( 59.10,      8) ( 67.10,      8) 
                         ( 74.10,      8) ( 77.10,      8) ( 79.10,      8) 
                         (368.35,      8) 

[MSZones]

MS Source                : 230 C   maximum 350 C
MS Quad                  : 150 C   maximum 200 C


                             END OF MS ACQUISITION PARAMETERS


                              TUNE PARAMETERS for SN: US10481367
                        -----------------------------

 Trace Ion Detection is OFF.

 EMISSION    :      14.833
 ENERGY      :      69.922
 REPELLER    :      22.081
 IONFOCUS    :      75.922
 ENTRANCE_LE :      12.000
 EMVOLTS     :    2376.471
                               Actual EMV  :    2376.47
                               GAIN FACTOR :       7.30
 AMUGAIN     :    2023.000
 AMUOFFSET   :     129.000
 FILAMENT    :       2.000
 DCPOLARITY  :       0.000
 ENTLENSOFFS :      15.310
 MASSGAIN    :     279.000   
 MASSOFFSET  :     -12.000   

                           END OF TUNE PARAMETERS
                      ------------------------------------



                              END OF INSTRUMENT CONTROL PARAMETERS
                              ------------------------------------

